Information of 4 Analytical Chemistry Experiment Books

Topic: Analytical Chemistry Experiment/Chemical Experiment Series Textbooks in Colleges and Universities

ISBN: 730703753

Authors: Experimental Center of School of Chemistry and Molecular Science, Wuhan University.

Publishing House: China Traditional Chinese Medicine Publishing House

Pricing: 12

Page count: 250

Release date: May 2003-1

Version: 1

Format: large 32 format

Packing: paperback

Introduction: This book is one of the "Tenth Five-Year Plan Textbooks for General Higher Education".

This book consists of the first part (chemical quantitative analysis), the second part (instrumental analysis) and the appendix part (commonly used analytical instruments, etc.). ) and Appendix 4. This book contains 10 1 experiments, including 32 chemical quantitative analysis experiments (including 2 English experiments); 69 instrumental analysis experiments (including 2 English experiments); The appendix includes analytical balance, common spectrophotometer, common chromatographic analysis instrument and the consulting method of Satler standard spectrum.

This book carries out the spirit of "three basics" and "five natures", meets the needs of analytical chemistry teaching, and is systematic, comprehensive, novel and concise.

This book, together with Analytical Chemistry, Selected Theories of Instrumental Analysis, A Concise Course of Analytical Chemistry, Analytical Chemistry Problem Sets and Analytical Chemistry Multimedia Teaching Software, constitutes a three-dimensional series of teaching materials for analytical chemistry.

This book can be used as an analytical chemistry experiment textbook for undergraduates majoring in pharmacy, pharmaceutical engineering, traditional Chinese medicine, pharmaceutical preparations, biochemistry, chemistry and chemical engineering, and also as a reference book for analysts.

Directory:

The first part is chemical quantitative analysis

1 Chapter Basic Operation of Analytical Chemistry

Experiment 1. 1 Basic operation of titration analysis

Experiment 1.2 basic operation of gravimetric analysis

Chapter 2 Analytical Balance and Weighing

Experiment 2 1 weighing exercise

Experiment 2.2 Performance Inspection of Balance

Chapter III Acid-base Titration and Non-aqueous titration

Experiment 3 1 titration analysis operation exercise

Experiment 3.2 Verification of Capacity Instruments

Experiment 3.3 preparation and calibration of hydrochloric acid standard solution (0. 1mol/L)

Experiment 3.4 Content Determination of Medicinal Borax

Experiment 3.5 Determination of Medicinal NaOH Content

Experiment 3.6 preparation and calibration of NaOH standard solution (0. 1mol/L)

Experiment 3.7 Preparation and Standardization of Sodium Hydroxide Solution

Experiment 3.8 Determination of Acetic Acid Content

Experiment 3.9 Determination of Benzoic Acid Content

Experiment 3. Determination of HCl+ in 10 mixed acid.

Experiment 3: Preparation and calibration of perchloric acid standard solution (0. 1mol/L).

Experiment 3. Preparation and standardization of12 perchloric acid

Experiment 3. Determination of13 sodium salicylate

Experiment 3 14 determination of diphenhydramine hydrochloride.

Experiment 3. 15 Determination of Ephedrine Hydrochloride

Chapter 4 complexometric titration

Experiment 4: Preparation and calibration of EDTA standard solution of10.05 mol/L.

Experiment 4.2 Determination of Water Hardness

Chapter 5 Redox Titration

Experiment 5. 1

Preparation and calibration of standard solution (0.05 mol/L)

Experiment 5.2

Preparation and calibration of standard solution (0. 1mol/L)

Experiment 5.3 Determination of Vitamin C Content (Direct Iodometry)

Experiment 5.4 Determination of Copper Salt (Displacement Iodometry)

Experiment 5.5 Determination of Glucose Content (Indirect Iodometry)

Experiment 5.6

Preparation and calibration of standard solution (0.02 mol/L)

Experiment 5.7 Determination of Hydrogen Peroxide Content

Chapter 6 precipitation titration and gravimetric analysis

Experiment 6. Determination of chlorine content in1chloride (indicator method)

Experiment 6.2 Determination of chlorine content in chloride (ammonium ferrous sulfate indicator method)

Experiment 6.3 Determination of Crystal Water of Barium Chloride

Experiment 6.4 Determination of Sodium Sulfate

The next instrumental analysis

Chapter VII Potentiometric Method and Voltammetry

Experiment 7. 1 Measure the pH value of the solution with a pH meter.

The method of measuring pH value of solution with pHS-2C acid meter is attached.

Method for determining pH value of solution with II-25 acidity meter

The method of measuring pH value of solution with PXSJ-2 16 ion analyzer is attached.

In Experiment 7.2, the chloride ion concentration was measured with a chloride ion selective electrode.

Preparation method of chloride ion selective electrode

Annex II Usage of Model 25 pH Meter for Measuring Electromotive Force

Experiment 7.3 Performance Test of Fluorine Ion Selective Electrode and Determination of Fluorine Ion Content in Water Sample

Experiment 7.4 Potentiometric titration of phosphoric acid

Experiment 7.5 Calibration of 12 standard solution (0.005mol/L) by never-ending titration.

Experiment 7.6 diazotization titration of sulfadiazine (never stop titration)

Experiment 7.7 Karl Fischer Moisture Determination (Never Stop Titration)

Experiment 7.8

Determination of conditional potential by electricity (drawing method)

Chapter VIII Ultraviolet-Visible Spectrophotometry

Experiment 8. 1 Drawing of absorption curve

The usage of 72 1 spectrophotometer is attached.

Experiment 8.2 Determination of iron content in water by o-phenanthroline spectrophotometry (standard curve method and standard comparison method)

Experiment 8.3 Performance Verification and Use of UV-Vis Spectrophotometer

Experiment 8.4 Determination of Vitamin Injection

Experiment 8.5 Determination of Absorption Coefficient of API

Experiment 8.6 The contents of sulfamethoxazole and trimethoprim in compound sulfamethoxazole tablets were determined by dual-wavelength spectrophotometry.

Experiment 8.7 Determination of Baicalin and Chlorogenic Acid in Yinhuang Injection by Dual Wavelength Computational Spectrophotometry.

Experiment 8.8 Determination of Caffeine in Anaka Injection by Derivative Spectroscopy

Experiment 8.9 Determination of Quinine and Sodium Benzoate in Nourishing Water by Ultraviolet Absorption Spectrometry

Chapter 9 Fluorescence Analysis Methods

Experiment 9. Determination of vitamin content by1fluorescence method.

Experiment 9.2 Determination of Quinine Sulfate by Fluorescence Method

Attached 930 fluorescence photometer and its operation method

Chapter 10 infrared spectrophotometry

Performance check of infrared spectrophotometer in experiment 10 1

Experiment 10.2 infrared absorption spectrogram

Chapter 1 1 Atomic Absorption Spectrophotometry

Limit test of impurity potassium salt in experiment 1 1. 1 heparin sodium.

Experiment 1 1.2 atomic absorption spectrophotometry was used to determine the magnesium content in drinking water.

Experiment 1 1.3 Determination of Zinc in Hair

Experiment 1 1.4 determination of calcium in water by flame atomic absorption spectrometry-standard addition method

Chapter 12 nuclear magnetic resonance spectroscopy (teaching)

12 1 performance inspection of nuclear magnetic resonance spectrometer

Drawing of NMR Spectra of Menthol in Experiment 12.2

Experiment 12.3 NMR * * * vibration method was used to determine the tautomerism and content of ethyl acetoacetate.

Drawing of NMR vibrational carbon spectra (COM and DEPT spectra) of menthol in experiment 12.4.

Chapter 13 mass spectrometry (teaching)

Performance check of mass spectrometer in experiment 13. 1

Experiment 13.2 mass spectrum of phenacetin

Experiment 13.3 Mass Spectra of Unknown Organic Substances

GC-MS Analysis of the Mixture of Toluene, Chlorobenzene and Bromobenzene in Experiment 13.4

Experiment 13.5 analysis of volatile oil from Ligusticum chuanxiong by gas chromatography-mass spectrometry

Chapter 14 classical liquid chromatography

Experiment/activity determination of kloc-0/41alumina (column chromatography)

Experiment 14.2 The content of sodium citrate was determined by ion exchange chromatography (column chromatography).

Experiment/determination of activity of kloc-0/4.3 alumina (TLC)

Experiment/Activity determination of KLOC-0/4.4 silica gel (adhesive board)

Experiment 14.5 Impurity Inspection of Triamcinolone Acetate (TLC)

Experiment 14.6 The content of inosine injection was determined by paper chromatography (ascending expansion method).

Experiment 14.7 phenformin hydrochloride impurity limit detection (paper chromatography downward expansion method)

Experiment/Isolation and Identification of Proline and Hydroxyproline from KLOC-0/4.8

Experiment 14.9 the content of ursolic acid in Liuwei Dihuang pills was determined by TLC scanning.

Chapter 15 gas chromatography

Experiment 15 1 Preparation of Gas-liquid Packed Column

Performance check of gas chromatograph in experiment 15.2

Experiment 15.3 determination of common chromatographic qualitative parameters and content determination by normalization method.

Experiment 15.4 Separation and Identification of Benzene, Toluene and Xylene and Applicability Test of Chromatographic System

Experiment 15.5 the ethanol content in wine or tincture was determined by internal standard method.

Experiment 15.6 Determination of Trace Moisture

Experiment 15.7 determination of relative content of two butanol isomers

Experiment 15.8 Determination of Optimum Carrier Gas Velocity

Experiment 15.9 determination of volatile oil from notopterygium incisum by capillary gas chromatography

Chapter 16 high performance liquid chromatography

Experiment 16 1 Performance check and chromatographic parameter determination of high performance liquid chromatograph.

Experiment 16.2 the content of prednisolone was determined by internal standard method.

Experiment 16.3 the content of paracetamol was determined by internal standard comparison method.

Experiment 16.4 the contents of norethindrone and ethinylestradiol in compound norethindrone tablets were determined by correction coefficient method.

Experiment 16.5 the content of cefaclor was determined by external standard method.

Experiment 16.6 The impurity limit of ciprofloxacin hydrochloride was checked by normalization method.

Experiment 16 7 HPLC separation of caffeine and benzene mixture

Tetrahedral optimization method of mobile phase in experiment 16.8

Chapter 17 Capillary Electrophoresis (Teaching)

abstract

Experiment 17 1 performance test of capillary electrophoresis instrument

Experiment 17.2 Qualitative Analysis of Tincture

Experiment 17.3 qualitative analysis of main components of cordyceps sinensis

Quantitative analysis of three components of compound hypotensive tablets in experiment 17.4

Chapter 18 Flow Injection Analysis

Performance check of flow injection analyzer in experiment 18 1.

Experiment 18.2 determination of iron content in tap water

Experiment/determination of the content of kloc-0/8.3 epinephrine hydrochloride injection

Experiment/determination of sulfadiazine content in kloc-0/8.4

19 chapter thermal analysis method

Experiment 19. 1 Determination of the purity of nifedipine by DSC thermal analysis technology.

Common analytical instruments and reference methods of Satler standard spectrum

Chapter 20 Analytical Balance

20 1 weighing principle of analytical balance

20.2 Classification of Analytical Balances

20.3 Structure of analytical balance

20.4 Installation and adjustment of photoelectric analytical balance

20.5 Measurement Performance of Analytical Balance

20.6 Usage Rules and Weighing Methods of Analytical Balance

20.7 weight correction

20.8 microbalance

20 9 electronic balance

20 10 balance room rule

Chapter 2 1 Commonly used spectrophotometer

2 1. 1.722 visible spectrophotometer

2 1.2 75 1g ultraviolet-visible spectrophotometer

2 1.3752 ultraviolet-visible grating spectrophotometer

2 1 4 756MC ultraviolet-visible spectrophotometer

2 1.5 UV-9 100 ultraviolet-visible spectrophotometer

2 1.6WFZ800 ultraviolet-visible spectrophotometer

2 1.7mpf-4 fluorescence spectrophotometer

Usage of 2 1.8 960 fluorescence spectrophotometer

2 1.9 7650 infrared spectrophotometer

2 1. 10 1703 Fourier transform infrared spectrophotometer

21.11wfx-1d atomic absorption spectrophotometer

21.12 p-E2100 atomic absorption spectrophotometer

2 1. 13 shimadzu AAS-670 atomic absorption spectrophotometer

Chapter 22 Common chromatographic instruments

22 1CS-930 thin-layer scanner

Brief introduction of 22.2 CS-930 1PC thin-layer scanner

22.3 the use of general gas chromatograph

22.4 Mei Tian 7890 gas chromatograph

22 5 102G gas chromatograph

22 6 Agilent6890N gas chromatograph

22.7 Use of Universal High Performance Liquid Chromatograph

22.8 the use of Hitachi L-7 100 liquid chromatograph

22 9 agilent1100+000 high performance liquid chromatograph

Brief introduction of 22 10 simple capillary electrophoresis instrument

22.11GCMs-qp5050a gas chromatography-mass spectrometry.

Chapter 23 Reference Methods of Satler Standard Spectra

23 1 Classification of Satellite Standard Spectrum and Index

23.2 alphabetical index of names

23.3 molecular formula index

23.4 chemical classification index

23.5 spectral line index

23.6 chemical shift index

23 7 C- 13 NMR peak index

appendix

Appendix I International Table of Relative Atomic Mass (1999)

Appendix Ⅱ Table of Common Relative Molecular Mass

Appendix III Common Indicators

Appendix IV Preparation of Common Buffer Solutions

Appendix ⅴ pH value of standard buffer solution

Appendix ⅵ Density and concentration of commonly used acids and bases

Appendix VII Drying and Application of Common Reference Materials

Appendix VIII Solubility product of insoluble compounds ()

Appendix VII Table of Standard Electrode Potential and Redox Pair Conditional Potential

Appendix X Cut-off Wavelength of Common Solvents

Appendix VII Analytical Lines Commonly Used in Atomic Absorption Spectrophotometry

Appendix chemical shift of residual hydrogen in deuterated solvents commonly used

Appendix ⅹ Ⅲ TLC stationary phase

Appendix X Common Stationary Liquid for Gas Chromatography

Appendix ⅴ ⅴ Gas Chromatography Relative Quality Correction Factor (F)

Appendix ⅹ Application of Stationary Phase in High Performance Liquid Chromatography

Appendix ⅹ ⅷ Properties of commonly used mobile phases in high performance liquid chromatography